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Separation and purification - EdexcelFiltration and crystallisation

There are different ways to separate mixtures, for example by filtration, crystallisation, distillation or chromatography. The method chosen depends upon the type of mixture.

Part of Chemistry (Single Science)States of matter and mixtures

Filtration and crystallisation

Learn more on filtration, evaporation and crystallisation in this podcast.

Filtration

is used to separate an solid from a liquid. It is useful for separating sand from a mixture of sand and water, or from a .

Filtration works because the filter paper has tiny holes, or pores, in it. These are large enough to let small and through, but not the much larger particles of undissolved solid.

Image gallerySkip image gallerySlide 1 of 3, One beaker contains a mixture of solid and liquid, the other contains a funnel with filter paper, Separating insoluble solids 1. One beaker contains a mixture of solid and liquid, the other contains a funnel with filter paper

Crystallisation

is used to produce solid from a solution. When the solution is warmed, some of the leaving behind a more concentrated solution.

Image gallerySkip image gallerySlide 1 of 3, A solution is placed in an evaporating basin and heated with a Bunsen burner, 1. A solution is placed in an evaporating basin and heated with a Bunsen burner.

To obtain large, regularly shaped crystals:

  • put the solution in an evaporating basin
  • warm the solution by placing the evaporating basin over a boiling water bath
  • stop heating before all the solvent has evaporated

After the remaining solution has cooled down, pour the excess liquid away (or filter it). Dry the crystals using a warm oven or in air.